By Professor Buzz
The only best e-book ever written at the manufacture of leisure medicines. Profusely illustrated, it covers the gear, suggestions and reagents utilized in the clandestine manufacture of unlawful medications. techniques for crystallization, chromatography, distillation and rate reductions are given for the subsequent varieties of medicinal drugs:
-- Hypnotics, Sedatives and Tranquilizers. additionally contains distinct directions for purchasing and making precursors. For informational reasons only.
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Extra resources for Recreational Drugs
If lightly with vaseline) pressure will not remain constant you have a hot leak and it must be fixed before attempting to plate perform the hydrogenation. Use soapy water to cover unions and valves to find the leak. After passing the pressure test, bleed off hydrogen very slowly by opening the discharge valve and watching the gauge closely, stop opening just as soon as pressure begins to drop. The discharge hose does not need to be high pressure, but it does need to be attached to a vacuum aspirator to evacuate the H2.
Another Zinc Reduction. Prepare amalgamated zinc by treating 50 g of zinc with 5 g of mercuric chloride as above. Agitate the activated zinc in 100 ml of methanol using an ice bath (ice baths are actually ice water baths). Add to the above solution a small portion of hydrochloric acid, then a portion of the nitrostyrene (20 g) in 200 ml of tetrahydrofuran. The acid (in small amounts) and the nitrostyrene solution are added alternately with cooling to hold temp below 50°. After the styrene is completely added, check to see if the reaction mixture has lost the yellow tint by spotting on filter paper; add more small amounts of HCL acid if you can see a yellow tint.
Mechanical devices can be rigged up to save your arm wear. When the pressure no longer rises or falls, this indicates that the reaction is complete. If the pressure drops too low, then you may need to add more H2. If the hydrogenation fails, you may try again at a higher temperature. Some formulas call for elevated temperatures. This can be accomplished by using an oil bath as shown in the picture on page 34. The H2 pressure will rise (unlike the operation at room temp) due to the rise in temp.
Recreational Drugs by Professor Buzz