By W. A. Plummer, S. T. Gulati (auth.), David C. Larsen (eds.)

ISBN-10: 146848267X

ISBN-13: 9781468482676

ISBN-10: 1468482696

ISBN-13: 9781468482690

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In addition, the dilatometer is designed to achieve rapid sample turnaround for quality control measurements in a production environment. To achieve this, design features are incorporated which minimize sample preparation time by relaxing critical size and shape restrictions on test samples. The length change measurement is based on a modified Michelson interferometer using a two-frequency HeNe laser and ac detection of fringes. The final critical alignment of the interferometer during sample installation is achieved by automatic computer control.

Removal of the compound from the bromine vapor led to intercalate desorption, which resulted in more dilute compounds. EXPERIMENTAL Thermomechanical Analysis Thermomechanical analysis (TMA) was performed by using a Perkin-Elmer Model TMS-2 thermomechanical analyzer, in which a linear variable differential trans former (LVDT) monitored the position of the probe which made contact with the sample. In TMA, one measures the expansion versus the temperature, as shown in Fig. 1, which was obtained during successiveexfoliation and collapse cycles of dilute graphite-Br2' Of interest is the mechanical hysterisis observed on cooling.

To aid in the current deve1opment, commercia11y-avai1ab1e equipment shou1d be incorporated wherever possib1e. TECHNICAL DESIGN A schematic diagram of the laser interferome'tric dilatometer system is shown in Fig. 1. The IEEE-488 interface bus has been adopted for all communication between the dilatometer and a minicomputer-based data acquisition system. The dilatometer system consists of the fo11owing components: Optica1 Interferometer A detai1ed schematic of the optica1 interferometer is shown in Fig.

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Thermal Expansion 7 by W. A. Plummer, S. T. Gulati (auth.), David C. Larsen (eds.)

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